31970-04-4, Benzyl 2,5-dihydro-1H-pyrrole-1-carboxylate is a pyrrolines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
a) To a solution of benzyl-3-pyrroline-l-carboxylate (compound 29. 1,10 mmol) in THF (15 mL) was added N-methyl morphline (22 mmol) and OS04 (2 mL of a 2.5 wtpercent in t-BuOH), and the resulting mixture was stirred at room temperature overnight. The solvent was removed ; the residue was dissolved in EtOAc (100 mL), washed with dilute aq. Na2S03, sat. aq. NH4Cl, and brine, and dried with anhydrousNa2S04. The solvent was removed and the residue was purified by column chromatography to give compound 29.2 in 55percent yield. EIMS (m/z) : calcd. for C12H1sNO4 (M+) +Na 260.1, found 260.1 ; 1H NMR (CD30D, 400MHz) : 8 7.31- 7.38 (m, 5H), 5.13 (s, 2H), 4.17 (m, 2H), 3.58 (m, 2H), 3.34 (m, 2H) ppm., 31970-04-4
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Reference£º
Patent; SUNESIS PHARMACEUTICALS, INC.; WO2005/44817; (2005); A1;,
Pyrroline – Wikipedia
1-Pyrroline | C4H7N – PubChem