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Group VI metal-promoted endo-azacyclizations via alkyne-derived metal vinylidene carbenes
The molybdenum-promoted cycloisomerization of terminal alkynes tethered to nitrogen nucleophiles is described. Reaction of N-carbamoyl alkynylamines with (Et3N)Mo(CO)5 affords cyclic enecarbamates. Similarly, cyclization of 2-ethynylaniline gives the isomeric indole heterocycle, although N-3- butynylaniline affords the cyclic metal azacarbene product.
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Reference£º
Pyrroline – Wikipedia,
1-Pyrroline | C4H7N – PubChem